i: r r ImperialTobacco LimitedlLimit6e r I- 1.1 j: [I r~ RESEARCH AND DEVELOPMENT DIVISION i: MONTREAL 1 i C 1 ia THIS REPORT HURT NOt BE COPIED OR SHOWN TO UNAUTHORIZED PERSONS, I I O to jl 00 03 ''"I"' " '' 10 lfJ Clit; PDF -!::!!::!!::!.f3 StlC.i: 0111 BOOK rII · INHOVAtrON JM(. FEB 1989 Clit; PDF -!::!!::!!::!.f3 StlC.i: 0111 Hcnday, JanUarY 30, 1989 IDDmX, ~------~e~ time T-MARKET eH Swlrs mane~ trends and neu prpducts (8lten) M BRn Bwilian market trends and new products jValpan) PS O Oernan market trends and new products (Klm) 30 UX nlddle East market I pmduct treads (CPus$s) ~O USA US market trends and new pro4ucrr (Alehl) 30 LUNCH BREAK R15 ~uaralian market trends and new products [BiCkhdf) UN Caoadillo market trends and new products (LlblPnd) (5 UK Hew BIT(UKE) products and launenes (eous~ns) 20 D Possible influences df the EEC single market on product deve~apment after 1942 (Kbhn) IS UK Uk 7rajeet 01OBE - Suney oi eempeot~ve product dS strategies (erellln) rI: -LEAF~PROEESS CH Important pnnclples to keep in mind when dcslgnlng cigarette leaf ncipes (8tron) Clit; PDF -!::!!::!!::!.f3 StlC.i: 0111 I _1_ Tuesday, January J1, 1911 Approx. I----~I~ tins fI · LEAP C PROCESS~ (eontinued) USd Oevalopments in leaf grades (alaekl (5 BPA Brazilian Onenta~l tobacco (Ollvsira) 30 USI, Leaf rs9ularorl Issun (BlaB) 30 BRli Characteristics of Coaun tobacco cured like 20 flubcured (Ollvslra) USA aeveloanrs in eostngs (Chakraborty) 20 UK Pmjcct ~~RK - Evaiulfion of the p~ducr Dersntial of HYO thigh veloctty drying) mated bland 15 eqonents tSteDhenson) O Product advantages In using HtD thigh t#nperafure drytng) processed tobacco (2iwnenann) BPA Casings and fidvan - New d8lllo9n~nrs (Olivlira) 30 USA SOS status (Rlehl) LUNCH BREAK USI tmpr3verral of expanded Eocaeeo (8lacki IS UX Projeett RIii and Il(fEeH. SDibaff technologY fn tha OEER process (Stephcnson) uSn I~nia disposition In ~a~lbom (ehakraborty) 20 CH Haryland tobacco eharactef~st~G5I properties in a blena, New sources of supply (81zon) 15 III- rNNOVAtIOH Uli Hm product coneepr~ (iocluding AIRBUS) (Riehl) 21 S~03 UX Projects FIIT and HINIC aaveteooent of reduced l5 ~3 tar delivery 0r:ducts (Crtllin) UM Develb#nen with Y1 tobacco (Blafk) IS Clit; PDF -!::!!::!!::!.f3 StlC.i: 0111 weanesday, February i, 1989 APDrOX, time IIr - rNNOVlfION (Continued) I~ - D Fitter additives for reducing smoke nicotine deliveries (KLn) 20 USA Low nicotloe pmduetr (Cnsknbcrty) 15 0 Consumer test results on ultra low delivery brands and products with hOllCY tube filters ~Kahn) US~i Filter aadlllves (Chakraborty) 15 BIU Smoke of cigarettes with taste and aroma ct tropical fruits (Oliveiral 20 eAH Project S~STURN - I~valeFcnant of flavored cigarettes (Smith) O Some preliminary results on paoirossy type prototype cigarettes for reducing sidestream snake emissions (n6hn) UK Project LESS · Development of low sidastraan products (Stapnenson) 45 9RA Effect of Virginia and Burley blends on cigarette smoke deliveries of N-n~trosamlnes (Otivelral 30 LUNCH SRUK UN Project YISA - low ridestrsan (KBrf~~) 30 BRA Reduction of unpleasant cigarette butt odor In ahtrays (Olivelra) 20 UK Project LncM · Bland and cigarette design influences mainstream biological activity (CrelllnJ 45 · eH Development of a a mg cigarette, project Kryoton 15 (Blton) IV - GENERAL O 3Rd Ouallty insoection system cvolpen) 20 0 eiqllrerle biPdeglade~lllty (KBhn) 30 q Clit; PDF -!::!!::!!::!.f3 StlC.i: 0111 rhlrlOll, Fdn~rlr %I) #m. tt· IV-GENE~L (Conftnucd) -~c" 8~ STORK 3r3Jlet. Rlstruclu~ng of tko P'~uet Dovoloeont sylta rit~n Sculn Crut lVolpdnl p IYB ~I~Mldka nrocnsa h' "Y p~ldl 8~~) II GRtUP · Otlcusrion on tH fcliowing twic~ - P~uZ pu~lltt II oorcidvod by bl eoa~rr, Rroduot b~~ll - he deli IlrLttnJ tton~( conaumsr v#tl In~ oroduot spKtrtc~flcnlt - grnll of ~~ct tnntlnS *tlcb~ll, Im the ull of u(oort in-houll lnekllrs a odnsunor or~tu~rlol, (eantl on 'Molllurvmnt of tooto ch~r~cElr ~th con~ar Dm~~ ~ b Km"l - Procadursl or procll~a~ usod to Idmtlly now product Ppponunlttas~ eV do you dtcido to wor4 on projlct X dr V1 Whlt guld~nel do you rsellv~? LUICH 81~1 G~~P Vhat 4svs we lslrnldl Yhor hna ul Iceapllshd! WhlCh lnd~ Ln thl lnoat pr~lslng for thl luturo? Yhlt work prlorltlll de uo ncrad! ClibPDF - v~~fastio.soni (y , Idl~ oa~l Mcl~~( PIII (Rl~hl) O O O 9 ClibPDF - v~~fastio.soni NEW PRODUCT CONCEPTS PRODUCT RKXIIRPrlENTS SOURCES OF IDE4S CURRENT d NrURE PROJECTS AIRBUS c c (x: c Clit; PDF -!::!!::!!::!.f3 StlC.i: 0111 PRODUCT REQUIREMEKTS NEW PRODUCTS MLCS[: (~)IE HIGH Qu~n"·l I MEE~ CONSUMER NEEI~ (ADDRESS CONSUMER CONCERNS I BREAK THROUGH lu14W(E~F~4~E CWT~ER Clit; PDF -!::!!::!!::!.f3 StlC.i: 0111 SOURCES OF IDEAS (PADINNC~PiTION ACTFKXIi I CAPW ( F)I~LRKmNGIMllffKET F~ESEARCH · UUIRASUM ULTRA · IMF#IA (NfEJ PRODIJ~TS PLANNING GF#WP MULTIPLE M~N~S -MENMOL. BWDGE (COMPET[T~VE PC~T~YTTY AIRBUS Clit; PDF -!::!!::!!::!.f3 StlC.i: 0111 Isl a, r dE t I~ r ~I ~-~J II ClibPDF - v~~fastio.soni PIB1I[1 lilBUI bBlt[TIYt rsovrff A Sn0rlm ~rrctE ulcH: ~ fif~0 1001(S, FEELS CHD QUALIFIES ~ )1 t~t~EnE PRdVrMS d~l m; urcot~rE By STANDARD ~EtHODS PRaVrMS ACIEP'TABLE ~~S'TE tHAWGHOU'f ~HE S~OKrNG ~R6CESS PIIOVIDES P 'TOBAC[O COnaUST~ON PRODUCTS ~N 'IHE MrrS~REI~ YHEY fllfY(EP, IE)IVES DEBRIS SrnIUR ~O MAT OF r.~MWTIOIIAI [rt)StETTE O(( BASICALLY REMAINS UNCHAYGED IS YI'TH PRMIER ~~B~glE ~Pr~b~S · ( GIVES ~ WFEHSI~ SrMStREEn tiIVES VISUAL S1Gn OF SIKIKIWE SfA~US 1S'ftB Y~E: ( IS Mrl~e~UrYOIBLE Clit; PDF -!::!!::!!::!.f3 StlC.i: 0111 QRREN[IESE~CH~S ( Modfied ~ ~ialiana~ Fwnace) Cwlceniric (Mo\n~g Fu~nace) ( SeqxnSd ~ ~$ ClibPDF - v~~fastio.soni $ "h03WH3 P 21 III ~xwls~ O 3~1Rg) ~wm Ba iil t~M ~3fh8a~' II ill ~;· ~BM ~· ClibPDF - v~~fastio.soni CONC~NIWC MOVING n854CE ( Fuel too hot ( Insukstjan does not protect core. TObOCCO bums, ( Pro~k~c~s hot messy deb~s. ( Not easi~ flickable. ( Not responsive to puffing U Clit; PDF -!::!!::!!::!.f3 StlC.i: 0111 W Z ZQ gB Clipj: r, I I i' I I iii i I !I I C C C: Q C C: e; Clit; PDF -!::!!::!!::!.f3 StlC.i: 0111 RESPONSE SEQUENT~G41 MO\I~NG RIF~WCE De~ers nicotb~e if there is con~ct~e heat tronsfer from the fuelto the tobacco, but · Produces hot messy debris. · Not flickoble. Try'u~ ~ determine ii con de~wer suffiden~ nicotine without conduction. Clit; PDF -!::!!::!!::!.f3 StlC.i: 0111 ·_ AIRBUS STATUS BY rSIARCW'89: · DETERMINE OPENINGS IN RIR Rr\TPII c~ja, · DISCOrm NE~UMSIIL~ION COMBRI~QK~I FOR ELUS MPE DESIGN (BaWj · mABUSH (X~NMTIONS FOR f~tWIOWNKXTnNE S[C~PP~G (BARIKE· FWDO Clit; PDF -!::!!::!!::!.f3 StlC.i: 0111 UK Pmjsets FELt ~nd WINIC. Oedopnt Of rsducad f8r dlltvlry produets, (enllln) ~lkallne sRoko I) hanhlr and ht~her ~~Rpact, Clit; PDF -!::!!::!!::!.f3 StlC.i: 0111 __ Prejecls: FElt ad HlNle Ptojoot: FELt s ~ b# ht in many morkofo thoro n o jgay nombor of fog l#r lmokors ~o ruY like k swiIoh ~ low t p~u~ buI ~at mwe ina n~ ~+~ul 6 notprovide I requimd Iml dterJMy ~5. h ud FEL'T Cb · (1) GPeoverp[adical~~LI~IL~~d lla ehara~t~is~cJdl mo PMWNF p~~4 n4 hdq idsnbfied La, (1) o*hil+·~a~l~dlJpn mutsstnmetch 1~~1r~Ob14 mgPMWNF)oroducts ~Y4~~ dLad ~ IC~bn eMiuated I~~dt; Y us at b6, he ur d · ($ JklR,fiBR (b) Yghor iovels ofoxpandodtobac(# incDrpora6nof hi9h nlcotinegradss aR deemed b be hi most lueees~ful qproacbes.. ~ SoeoIol Rr (~l~n U,K. a~~ m ehossn ao $a A nun~ of design mutes we(e eveluated whieh olpY · (bc) ebwe, plus (d) Bldq modificd6on fo he blond od (~ roduced stsfn on~nt in vsrleus ombidons. A mge of It~ot~vens~on cnntbnotlenJ were iao ovslueted. A ~lmLh in s&H 8~ h b( Ip PYq wes 3# ~1 I design mute ~i~ mPpry high B oontonl eulley modifIwtion to hi Yln4 ~doed sLrn oonLnt and Hgh fiasr prossuro dfpplrsduad wdlden. Rojsd: HIHIC me Wqa of onla behaviad studies iniy ~ f mast Jmcksrs, ~pdn+C as mo of ~~ is u Ihllur rlguiremoot The tosk of MIMIC is to prwide hb, but h mnm~a 1 minimum feasible ~b yet rYI an accePtabiiIty mY with 811 Cut a ma PMWNF, 0919 6~01. sY using F~gC Ynb, s rnaehenirs ndlar mY re ~lred using I design which d~td 6 mt PMWMF and P7 mg nieotine; impact and initant asnljonl r ~g~nm 81 Cut Impd in p4cdr b are to depend not only uoon ddn delivery end smoke pH but also upon nicotine one~an h ter. O ClibPDF - v~~fastio.soni Impaetlinitab~n match (wib~out flavour loss) was achieved by addition of add ameliorants to the existing blend 1% add·on of lactic add achieved be closest match to target p~duet A detailed consumer test (Prajeet: W~A) is being conducted with ~50 Silk Cut srnckers which involves a range of lactic acid levels. 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TREATMENT WITH ACID AMELIORANTS -· IMPACT AND FLAVOUR MATCH i. : 3, i, 2, 34b ADD-ON OF LACTIC, CITRIC, TARTARIC, MALIC ACIDS 4, 1% LACTIC ACID PREFERRED (IMPAeT MATCH NO OFF-TASTES GENERATED) 1 OMEGA PANEL MATCH WITH SILK CUT ON I MECHANICS L IMPACT - IRR!TATION ,fLAVOUR AMPLITUDE Clit; PDF -!::!!::!!::!.f3 StlC.i: 0111 w P: ,II Z(1 Z UI IL ~Z C w OY O p: (10 O O P 05 Z 2 V1 0~ P O Ob O L~ I~ r Z Ew I11 cn i~~ o m 111 b· p~ I1I O la r Z~ p r ~L P O C] d~1 O wn: cn r a O re u, mP Z cn ~e d a O P E O o: rr ee· w c r W P LU UI P )d ~ E u! z (I Co , u, O I ~O Z ~·1 C· ~Z O Z O F O > w rr w lu O r ) ~ ~ P~~ ym u) X P O d >~ (Z ~rlW I)) CO O I I) O m 1Z 5 P 4 ~ P: ~) ZLT UI r W Y 2P ~W Ww O> Ow u, PO O O~ em cn > O Y1~Wm c; ~ mP O Clit; PDF -!::!!::!!::!.f3 StlC.i: 0111 USA Oevelogaonts with Y1 tobacco (8lack) Cwrments: The oain DredualPn of Y1 tobacco Is actually fn Btar1l, but B i W wants to further develop other lacattonJ such aJ tlabsbwe, euatanala .,, (Ses p,d) D1Wetent levels of inclusion of Y1 tobacco won assessed internally (X ln blend: 0,10,20,30), The best results were achieved with lax Y1. Hlcotlne delivery at dlffsrent levels of inclusion: ~Y1 0 10 20 30 11 mg .83 ,89 ,95 1.01 6 ng ,56 ,63 ,19 Clit; PDF -!::!!::!!::!.f3 StlC.i: 0111 I W OC 3) O W LL W Z t- O O Z I I a o o co 03 w Clit; PDF -!::!!::!!::!.f3 StlC.i: 0111 Y1 us. STANDIWO R;\I~WEN Mc~ 944 Y1 T, AUOLMD 42 75 T.SUGAR lee 1"5 Clit; PDF -!::!!::!!::!.f3 StlC.i: 0111 Cfl c~d ,4 O 3\r" 4:4 0·. O f W n: osJ (I) a t· 3 3 32 h c O \t I 5 O 2a d9 3 W II Eu. Clit; PDF -!::!!::!!::!.f3 StlC.i: 0111 'T~ENGS ~ ~ IE~a~F(B) ABO~T US~NG II MTFU SI~GCR OH ~C ~SHG QQEP SU~CCMC FUIX] COHSPNT~ I ~K1 SPECK C~CBT[E PROCESSING NEEMD~ ( USP(G Y1 LEK C~D Tlff OHY TO DEM1OP REA3I UP PROWCTS Clit; PDF -!::!!::!!::!.f3 StlC.i: 0111 BLEND COMPO~IPIT J6 FUE~FED 34~0t BUF~LEY 2~10 ORIE~ITCL 17X) EER 7,0 C#r 10~9 FGS~U 610 '1NCUII~S 2~k Y1 Clit; PDF -!::!!::!!::!.f3 StlC.i: 0111 a %?I W O!R W I, Z PP O d o r,rZb e O o I w o ClibPDF - v~~fastio.soni P4NS ~~ ~ ur~us 70/30 BCB9 DIFFEF~ENF RIIK~ INCOFIFdRIGIE ETX·21 O 10f~ UUPA OHY DESIG~t FBTER PRESSW1E DFK)P · F~CPW · VuCT FATE BLP1R 20X E1X·21 Clit; PDF -!::!!::!!::!.f3 StlC.i: 0111 O Filter aPditives for reducing smoke nicotine deliveries (Koehn) 1, Situation in C;eroany, Figures are printed on the pack: tar, nicotine, Internal 11911 ooinlcn: tolerance man value over either 12 analyses or 1/2 year not above 0,15 If printed figure is 0,7 otherwise we should print 9~, Harketfng in anst caries do not want to change figures because that also very often means to change the strategic poJttioning of that brand, 2, In recent tiles we scnetfps observed an Increase in smoke nicotine ~S?P~f an increase in far (or to a lesser degree for tar), 3, bewse In the pas: i~e~doe used Dlethyleltrate (301 Ly weight in triacatln which resulted in a 2,'13 inclusion level) for increased nicotine retention, Reen~tsma got a patent for this tnau~nt, In out trials with Dlethylcttrate we only found very low to no Ineraase in nlsotina retention. we believe that the weak acidity (~XIN5) is resPonsjble for that J, Objectives the existing squfpmant for the production of filter rods should be used, - the additive should work on cigarettes with 0,3 mg, smoke nicotine and above, the additive should be permitted for use according to Gernan regulations, low costs for the additive, - no influence on taste, Clit; PDF -!::!!::!!::!.f3 StlC.i: 0111 5, Results ruo different possibilities to apply organic acids to the tow. Anhvdric orocess 2 acids preferred: Halelc anhydride eftric anhydrlde Sclubillty in trlacetin: lleleic ~ 301 by weight eitric n,2g " Because the anhvdrido of an organic acid Is not allowed as filter additives It has to be converted Into the free acid, After adding water to the ~rlacatlnlanhydrlda solution the solution is stable/clear for appraxinately 3 hours before the acid is starting to pracipitata, Th time before the conversion Into the free acid Is nearly ceongleted is about 2 days, Analytical results is inclusion level bY weight gives a reduction of O,t ing smoke nicotine In full flavour products (0.9 · l,j pp nicotine), - 2X Inclusion level ~ 6,2 mg reduction In snwke nicotine, - c':ric acid gives slightly lower retention than maleic acid, beause of Its tewer acidity (citric acid pkii a 3,13, maieic acid pkl~ : 1,9), nleromlt]ed Acids To avoid the use of anhydrld acids and their eMNersi#l MI the filter and to make use of a broader variety of organic acids, Tartaric and nalie, one can apply the acids by spraying a suJpension of the wanted acids in triacetln onto the tow, The way to do that with the existing Iqulpmcnt Is by milling the acids to 8 particle site of less than 10 ynl with this particle site the aside an easily suspended in trlaceiln, The long ten stalllity of this suspension can he greatly improved by adding small amounts of Aerosi i, a pyrogenic sillca, O Clit; PDF -!::!!::!!::!.f3 StlC.i: 0111 Analvtioat Results SMI effect I the Anhydrlds Praeess for eltne end ~4lele acid, nalfe and tartaric acid less ~ff~ctlv~, cm Rlalg Oeereaoe In AtanSt~ level, ~ne~ku In nlldnu. lass ~ceaptabllItylPtelsrenu a~Pngsr full Ilavour snobn (no dffferenw for narlbam slmur In cdse of ha Illea), higher. accs9tabf I~ty ap3np low tar swk*, 111 other d~~ferancl~ (trrllatlon, ful~nJI) In ~xplalnsd by the lower strength rating, Oi scwslp? 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