'n REIPSOWUP Cft HA~ 2 ndATOUNnt WOE TO DR. S.R. EVELYN. rRON1 P.J. NICHOLL. $;EF PJN/Mj/46D-2. GATE 11th January, 1973. PCL SAMPLES FOR JANUS B3. B9 and B10 The lamina blends processed are summarized below Origin Grade 1 BO B~ B9 B10 % l Crop Crop % % rop % C rop U.S. EB2E 6.o6l 64 M2 E/GA- 6.06.1 61 6.09 6 o6 H2 E 6.o6 1 62 6.09 6:06 6.34 69 MF2E 6 061 62 5.68 6.o6 6.36 69 R2 E 6:o6 62 6.o9 6.o6 6.29; 68 RW 6 o6 l 63 6.09 6.o6 R3 W 3:o4 64 3.o4 3.04 AF2E 6.o6 62 6.09 6 061 BFE 6.o6 64 6.og 6:o6 ME 6.o4 6.06 M2 E 6.2o 68 HE 6.27 69 02 B 6.32 69 02 W 3.14 68 MFW 6.21 67 BFXB 1 6-32! 69 AF2E 6 31 68 BF2XE 6:331 69 Canada CM 6.o6 64 6.09 6.o6 CM2 6.32 66 CS3X 5.6o 68 Rhodesia RBD 12.12 63 12.17 12.12 RBE 6.o6 61 RBL 6.o6 61 6.09 6.o6 RAF 6.o9 6.o6 India IM 6.o6 63 6.09 6.o6 ID 12.12 64 12.17 Ix 12.12 Pakistan PKI 3.15 69 PK2 6.27 69 Korea BAL . 12.57 69 62 IS66001 BATCo document for Province of British Columbia 2 November 1999 -2- 19 a," WWNW DR. S.R. EVELYN. llth January, 1973- All PCL9 were made at Ajax by the Mark I PCL process i.e. three parts dryside materials to one part binder and 7.5% glycerol d.w.b. on product added. No physical data on the ma terials is available but there are important differences. PCL for B3. It was requested that this be made by normal Canadian process in which drY5ide materials consisted of .75% lamina waste and 25% winnowings and the binder was made from VSR stem. Thus, for the JANUS sample the dryside materials consisted of 75% lamina blend and 25% VS stem and the binder was made from VS stem. (In Canada the stem was sieved over ill. Oversize from mixed grades classed as VS; oversize from sand leaf grades classed as VS-1 and undersize classed as VSR.) The dryside materials were milled to 93.2% less than 270 mesh. PCL for B9. a3. For this PCL the dryside consisted of~lamlna Iblend. only The binder was made from Canadian flue-cured stem suppli.2r_ from the U.K. Gerlach additives were included as well as 7.5% glycerol. Target Glycerol Celacol 1-3 butylene Orthophosphoric and four levels were Target % -&ewmt% 7.5 7.7 t__ id~ _kj 10.0 10.0 glycol 12.0 12.2 acid 0.5 0.5 The lamina blend was milled to 78.4% less than 270 mesh. The sheet wasllgelled" in nature. PCL for B10. This PCL was made from three parts milled lamina blend and one part binder made from a new batch of Canadian flue- cured stem. At the time this was made it was commented that there was difficulty in achieving a "coarse enough flour" from the lamina blend, 90% passing 270 mesh compared with a normal 75% in production. It was stated that the sheet was denser than normal production (It should be noted, however, that the fineness of the flour was similar to that for the B3 PCL sample). Xt* BATCo document for Province of British Columbia 2 November 1999 now DR. S.R. EVELYN. Ilth January, 1973. For previous PCL samples reasonable agreement between found and calculated chemical constituents was obtained. This was not the case for this sample and the discrepancy could not be accounted for :- Calculated% Found % Nicotine alkaloids 1.73 0.89 Total sugars 15.8 11.8 Reducing sugars 12.5 9.6 Ash 10.1 16.3 Water solubles 45.7 56.5 Calculated figures allow for 25% stem solubles in the binder - which is normal for Canadian PCL. c.c. Dr. D.G. Felton. C=) 110 BATCo document for Province of BritiSh Columbia 2 November 1999