8850,PF0 Technical Mernorandun-i CNN NO. TH.80-01-006 Subject Authors TO Circulation File Key words PROJECT GYPSY Mr. D.E. Creighton Dr. F. Haslam, R. A D. Department, Hillbwik. Project GYPSY V19' 1.004 RESTRICTED May be opened and seen a nly by the addressee and persons authorized by addresses. Date 3rd January, 1980. CONFIDENTIAL 10 Pr COF71ED OR qH(D\/VrJ 'TO PERSONS Cr1\ cc cc BATCo document for Province of British Columbia I November 1999 LOW TAR TO NICOTINE RATIO CIGARETTES The objectives of two projects, GYPSY and ROMANY, are to design and manufacture cigarettes with low tar to nicotine ratios. When the projects were started in 1976-1977 cigarettes with the greatest sales in the U.K. had delivery ratios in the region of 14-18:1 (1.5-1.8mg nicotine). At about this time the results of a three month study of human smoking patterns were analysed in GR&DC (Report No. RD.1530) which reached the conclusion that nicotine was a major determinant of smoking behaviour. The view was expressed that there could be commercial advantages in the production of cigarettes which. gave less tar for the same delivery of nicotine, as such cigarettes would occupy lower positions in the league table but be as satisfying to the smoker. Dr. M.A.H. Russell expressed the view more dramatically as "Smokers smoke for nicotine and die for tar". He also published in a medical journal a paper expressing this view more scientifically but still speculating that low tar to nicotine delivery ratios would be to the long term advantage of the smoker who could not give up smoking altogether. He recommended Carlton King size cigarettes with a tar to nicotine ratio of 10:1. An examination of the cigarette design handbook suggested that if a high nicotine delivery blend was used together with a high efficiency filter, high paper permeability and filter tip ventilation, then tar to nicotine ratios of better than 10:1 could be designed. It remained to be seen whether they could be manufactured and whether they were acceptable to smokers of conventional cigarettes. Effort was directed in Product Development to design cigarettes using tobacco blends similar to the lamina portion of Capstan Full Strength (Table 1). A number of versions were BATCo document for Province of British Columbia I November 1999 produced and evaluated (KIOI-KI33, Table 2). many of the designs were rejected as they had very high impact but low mouthfeel and poor smoke texture. The smokers felt that they did not get a good mouthful of smoke but tended to become 'woozy' towards the end of a cigarette. Two cigarettes K129 and K113 were considered by the PDG to be worthy of further testing. As our thinking in Southampton and that of Dr. Russell at the Institute of Psychiatry seemed to be running on parallel tracks, Dr. Russell was approached by Dr. R.E. Thornton with a view to setting up a collaborative study. Dr. Russell was agreeable and cigarettes with a tar to nicotine ratio of 7:1 were supplied for what became known as "Dr. Russell's Safer Cigarette Study". This cigarette was also made from the high nicotine blend (Blend Rl) fitted with a dual filter, porous tipping and high permeability paper (see Table 3). The smoking qualities of this cigarette were not good when compared with a cigarette of more conventional blend and design (Table 3)(similar tar level but normal f16:11 tar to nicotine ratio). Due to the high overall level of ventilation the test cigarette was difficult to light, with initially a very low delivery of smoke. The cigarette took 12 puffs to smoke under standard conditions compared with 10 puffs for the control cigarette with more conventional design. The taste and flavour characteristics of the low tar to nicotine ratio cigarettes were judged to be poor. Design studies continued in Product Development where ventilated tipping was used in place of the porous tipping. Blend design philosophy was to use high nicotine delivery tobaccos. Some of the tobaccos used in earlier trials were upper stalk position grades, which are usually reserved for pipe tobacco blends. it was felt that it could be these upper stalk grades that were CC) CO BATCO document for Province of BritiSh Columbia 1 November 1999 upsetting the taste and flavour and impact-irritation balance aspects cf the smoke. Three new blends (NG1, NG2, NG3, Table 4) were formulated by Leaf Department which contained none of the tip grades but all cigarette quality leaf grades from the 1977 US crop. Due to climatic conditions the 1977 US crop was exceptionally high in nicotine but of poor smoking quality. (It was, however, realised that there was insufficient of this tobacco to support a brand.) A series of cigarettes were made, L500-L505 and M184- M186 (Table 5) from these blends. Tar to nicotine ratios of 7:1 were achieved but again the smoking qualities were judged to be poor, with high impact, poor smoke texture, high irritation and unbalanced taste and flavour characteristics. From these tests it was concluded that there was nothing inherently wrong with the use of the upper stalk position grades in the blend, but it could be that the target levels of 10mg tar with 1.0, 1.2 and 1.4mg of nicotine were essentially unbalanced. The design was changed to achieve a delivery with less than 1.2mg nicotine. it was also found in other projects where low tar delivery cigarettes were required that low tar to nicotine ratios could be achieved using conventional Virginia tobacco blends such as Blend 72 (Benson & Hedges) and Blend 48 (State Express) . The cigarettes made from these blends (MI81-MI83 and M417 Blend 48 and M414-416 Blend 72) had tar to nicotine ratios of 8-10 with PMWNF (tar) deliveries of 6-9mg (Table 6). These cigarettes were not judged to have gccd taste and flavour characteristics and had poor smoking mechanics. The advice of Leaf Department was again sought to provide a blend which ventilated well (i.e. maintains an acceptable taste balance at low delivery). Mr. I.R. Snowden of Leaf Department r"J drew our attention to the Swiss B & H Luxury Mild cigarette which ON CJO Oc BATCo document for Province of BritiSh Columbia 1 November 1999 had a delivery of 1. 4mq TNA, 12. 6mg PM14NF (tar to nicotine ratio 9 :1) . Consequently some B & H Luxury Mild blend (modified blend as in Table 7) was ordered and has been made into cigarettes which have tar to nicotine ratios of 7-10:1 with tar deliveries of 6-10ma (Table 8). These cigarettes have not been fully evaluated but initial taste and flavour reactions are the most favourable yet. D.E. CREIGHTON DC/A.H/E.1.004 3 rd january, 1980. cc BATCo document for Province of British Columbia I November 1999 TABLE I BLEND R1 c 1-, 2 15% C p. -, 5% R --- W 20% HZ-,,i 15% H 2 Z 5% A -7 --, E 7h% 17 7~% 15% K::L 10% Blend n-'cotine 3.4% Reducing sugar 15.6% Total Sugar 19.9% DC/AH/E.I.OC4 3.1.80 0- CO CDC C7 \ BATCo document for Province of British Columbia I November 1999 TABLE 2 LOW 7L.. TO NICOTINE RATIO CIGARETTES TOBACCO TAR TO FILTER PAPER TIPPING ROD TPM Pf1WNF NICOTINE CARBON NICOTINE LENGTH PERM, PERfl. LENGTH MONOXIDE RATIO MM Cu Cu MM MG MG MG MG U11 15 50 300 64 28 22 2.6 3 8.5 K109 20 50 300 64 24 20 2.1 13 9.5 Yd12 25 50 300 64 16 ja 1.6 NM 8.8 K121 20 50 600 64 15 13 1.4 11 9.3 K133 20 50 900 64 11 9 1.2 8 7.5 K107 15 120 300 64 26 21 2.4 12 8.8 K105 20 120 300 64 20 17 1.9 11 8.9 K108 25 120 300 64 14 12 1,5 10 8.0 K117 20 120 600 64 15 12 1.8 6 6.7 K129 20 120 900 64 11 -10 1.3 9 7.7, K103 15 200 300 64 22 18 2.0 10 910 K101 20 200 300 64 17 14 1.7 9 8.2 K104 25 200 300 64 13 10 1.4 12 7.1 K113 20 200 600 64 10 7 4_ 5.4 K110 20 50 300 60 23 19 2.1 10 9.0 K122 20 50 600 60 17 14 1.8 9 7.8 K134 20 50 900 60 14 11 1~4 7 7.9 K106 20 120 300 60 17 14 1.7 10 8.2 K118 20 120 600 60 11 9 1.4 6 6.4 1 K130 20 120 900 60 11 8 1.2 4 6.7 K102 20 200 300 50 15 13 1.5 5 8.7 K114 20 200 600 60 15 13 1.5 7 8.7 K126 20 200 900 60 10 8 1.2 3 6.7 BLEND RI WAS USED FOR ALL SAMPLES -:-.4 2.5Y/40,000 ACETATE TOW AND 3,000 CORESTA PLUGWRAP WHICH GAVE A BOUND PD OF 490mmK PER 120MM F11-77 ROD. DC/AH/E.1.004 3.1.80 BATCo document for Province of British Columbia 1 November 1999 T,L3 LE 3 CIGARETTES SUPPLIEZ TO DR. M.A.H. RUSSELL 8548Y 394B5 Blend R 1 72 Filter length mm 20 20 Plugwrap permeability CU 3,000 not porous Filter material !.!=n MYRIA 6mm CA CA Tipping permeability CU 900 not porous Tobacco rod length mm 64 64 TPM mg 12 13.6 PMr,4NZF mg 10 11 Nicotine mg 1.2 0.7 Carbon monoxide mg 6.8 12.9 Tar to nicotine ratio 8.5 15.6 DC/AH/E.1.004 3.1.80 c0 cc co BATCo document for Province of BritiSh Columbia I November 1999 TABLE 4 TOBACCO BLENDS NGI, NG2, NG3 OF 1977 US CROP NGI NG2 NG3 EE 10% 5 % - E2 W 5% 2.5% - HE 10% 5 % - HW 5% 2.5W - L2 XE 10% 12.5% 15% AF2E 5% 7.5t 10% AF2W 5% 5 % 5% MFW - 2.5% 5% D2 W - 2.5% 5% D2 E - 2.5% 5% CF2E - 2.5% 5% CF2W - 7.5% 15% CS3X 10% 5 % - CDC2 15% 12.5% 10% CR2 10% 10 % 10% CAF2X 5% 5 % 5% CRS 10% IG % 10% Blend NicotL%e 2.5% 2.95% 3.4% DC/AH/E.1.004 3.1.80 (Z) c0 CXD BATCo document for Province of British Columbia I November 1999 C) (1) .0 E (1) > 0 z T- m m E m 0 4) C.) S 0 L. CL L. E 0 V 0 IN-2168'M ClWi MS W W TA BL E 5 US CRO P TOR ICC OS IT H 1977 L5 00 L501 L502 L5 03 L5 04 L 505 f1184 K85 , W 6 To aAcc o B LE te %3 W 3 W 2 t o to t o NU FI LTER MA TE RIA L 2. 5y 4 G,0 09 2. 5Y 40,W0 2. 5Y 40, OW 2. 5Y 4 0,0W 2. 5Y 4 0,O W 2 .5Y 40,000 2.5Y 40,0W 2. 5Y 40, 000 2. 5Y L 0,0 00 FI LTER LE WU H M 2 0 213 20 2 0 2 0 20 20 20 2 0 PL LUAA P PE RM W IL ITY CU 5,0 00 5, (W 5, W0 5 ,O W 5 ,0 00 5, OW 5 , WO 5, 000 5, o oo BO UM P O FI LIE R Cjli -.(i 8, 4 911 8 .7 8. 8 3. 8 8 . f) 9.2 9 .2 9. 4 PA PER P ER ME MI LI TY CU 5 7 61 52 5 3 5 1 118 47 47 12 3 Ti ppiNG 0,4 B 3 R 4, ENK OW 44. ERT 6 811 0. Z 15,4,5 GENE 8 ti, (41A 0. LA 15, UCE 4, NE 5 0, 3 4 x FE R O, NK ow 4 x0,6 ERT 0, 3 4 x BE R O. NK ow 4 xO ERT .6 a M,0. MAL 15,4,5 MCENE K0 MAL ,15,4,5 MCENE 91 K ,0. DRY q 15, LIN ArE 4,5 E NE 0.4 D B 1 xO R EN R . YL K OW 4 xO. INE ERT 6 To BAcco R OD LE NG TH M 6 11 64 64 6 4 6 4 64 64 64 6 4 TP M vG 11 .6 1 5.3 1 9.9 15 .5 12 ,8 1 5,0 16.4 1 5.0 1 3 .0 RI O 10 .1 1 2.8 1 7.1 B .6 10 .7 1 2.4 12.9 1 2.4 1 0 .4 NI COTIN E VG 0. 92 1 .25 1 .611 1. 31 1. 23 1 .45 1.63 1 .59 1, 43 TA P TO Ni c0 TIN E RA TIO U . 0 1 0.2 1 0.4 10 .4 8 .7 8.6 7.9 7.8 7 .3 CA FW14 MO tJO XID E MG 13 .3 9.8 1 3.9 10 .1 9 .3 U.9 11.2 1 0,2 8 ,6 RJ VE FF NO WILA . TI N 2 10 3 .4 7 9.9 28 9.9 21 10 3 .3 4 10 3 .7 7 9.9 28 11.0 23 1 0.9 x 1 0 2 .6 7 E 4) 0 z T- m :5 E U) 0 0 %~.. 0 E 0 0 1022 1689 1 1- 00 D ELI VE RY CI PIAD TI TL E 6 OM CON VI3710 1 A L VI RG INI A BL I M E FR GAR EM fa 8 l K1 32 M8 3 M 17 M i ll PY 11 5 M 16 To a Ac co BLE W 1 18 1 13 48 4 3 72 7 2 72 F IL TE R WE RIA L 2 110 . S ,0 Y 00 * (-A U -IA ffAl o 11 M 010 Y )9 AN W 9, A 0541 0 NI 14 SE - 0 A 5410 N 164 WA 65 L65 M S6 WA 110 56 F IL TE R L ENG TH m 20 2 0 20 2 0 20 2 0 20 P LL 0 4RA P PE WIE M ILI TY (1J 51 w o - 5 ,( M - - - - B ou ND P D FI LTE R cm WG 9 . 7 8 10 9. 3 9 .3 8 . 7 7 .5 4 .3 P AP ER P E WF ABI LI TY CU 48 1 91 44 3 7 42 4 0 42 T IP PI NG 0. + I 44 DR BEN R .1 Y K OW 4. LINE ERT 6 4 M, MA 0. LA 15,4 UCE ,5 NE 0 3 .4 BE Ro 4. NK ws 40.6 ERT 41, IIA 0. LA 15,4 UCEN ,5 E l tl, tk O. LA 1 U 5,4,5 CENE 6 M q ,0. kLA 15 L)C ,4,5 ENE 8 P P U.1 kLk 5,4 XE ,5 NE T os Ac co ROD LE NG TH mm 64 6 4 64 6 4 64 64 64 T PM m 1 0. 7 9 .8 6. 7 9 .8 9 . 1 7 .9 7 .0 P1 .1 4f P r. 8 . 8 8 .2 5. 7 8 .3 8 . 0 6 19 6 .2 N IC O TIN E MG 0 .8 9 0. 92 0.7 2 9. 90 0 .6 4 0. 5 8 0 .64 T AR T O N ICO TIN E RAT IO 9 1 9 8 .9 7. 9 9 .2 12 . 5 11 . 9 9 .7 C AIl BO N M ONO XID E PIG, 9 . 6 7 .6 5. 6 5 .1 7 . 0 4 .7 2 .9 P V UF EN F T No ILA . T ION % 1 0. 29 6 10 3 .4 5 In. 32 6 10 4 .3 6 1 0. 38 9 11 5 . 9 1 1 1.6 66 CD TABLE 7 MODIFIED B & H LXURY MILD BLEND (SWITZERLAND) AF2E 3 AF2W 2 L2 XE 5 E2 E 6 H2 E 10 HE 5 HW 3 L1 XE 3 MF2E 6 TUE 5 T1 XW 3 B4 VT 2 BKBT 2 1 DS 2 US 4 CAF2 2 BCD2A 3 BCE1 10 WTS 24 100 DC/AH/E.1.004 3.1.80 00 BATCo document for Province of British Columbia I November 1999 M E 4) > 0 z qrl 25 m E (A 0 0 0 E 0 V 0 10221689") C ME VI T1 4 r WIFI SS B 9 11 L UX URY M IL D B LFJ D KA U R S B) S WI M 5. u M 51 2 M 5 B P 5 14 P5 15 M 516 M517 1,1 518 Tc B ACC O P JLE ND Sw l MO ss D B w Sw l j b Ss o Bm Sw i M s OD s BW. Sw i MO ss D B M Sw M is OD s W! Sw r is m s B &H Swi MDD ss m l S M wis ol) s R&H FI L TER MA TE RIA L 1 35 .8 , 5Y M) 1 35 . 8 ,0 5Y W 3 45 . , 5Y 000 1 35 .8 , 5Y n NL f V WA A% 24 AN 1 S4 1,41 77 M7 ANS tilA 492 747 A NS4 WA 7 W FI L TER LE ws TH Pit 2 0 20 2 0 2 0 20 20 20 20 PL U GWR AP PE NIE AB ILI TY CU 5 10 00 5 ,0 00 5 , U 5 , U - - - - Bo u ND PI) FI LTE R at WG 8. 9 8. 6 7 .6 8. 6 8 .3 8 .1 6.9 8 .0 P AP ER PER ME ABI LI TY CU 12 0 51 1 26 H 6 1 24 u9 m 45 T IP PIN G 0 A D B 2 X R E R O YL NY ow AX IN ER 0.6 E T O A D 2 X R BE R O YL NK ow AX-9 INE ERT .6 0 . 3 4 x BE O N Row ,4 x0, KERT 6 DA P 3 4 E N .44 KER .6 T 9 1, MA 0, LA 15, UCE 4,5 NE L1 1, MA 0. LA 15, UCE 4,5 NE LIM.,0 VAL .15 AUC ,4, ENE 5 SM M 0. ALA 15 uc A5 E NE T OB ACC O ROD LE NG TH mm 6 4 64 6 4 6 4 64 64 64 64 T PM 7. 2 8. 7 8 .4 6 .2 6 .8 U .5 12.3 8 .4 R I- If m 5. 8 7. 2 7 .0 5 .1 5 .6 9 .6 1011 6 .9 N IC OT INE MG 0 . 68 0 . 80 0. 76 0 . 74 0 .70 1 .14 1.09 0 .72 I AR TO N ICO TIN E RA TIO 8. 5 9. 2 9 .2 6 .9 8 8 .4 9.3 9 .6 C AP IM M ONO XID E MG 4. 8 6. 5 5 .7 3 .7 2 .9 6 .0 6.2 3 .1 P V UF EN F TIL No. AT ION Z 9. 4 9 9 9. 47 2 10 5 .1 0 1 0 5 .0 2 1 9.2 63 9 .6 41 10.1 41 9 .5 65